INTRODUCTION TO SOILS - A LABORATORY
MANUAL
SOIL 252L - Soils Laboratory
Department of Agronomy and Horticulture
New Mexico State University
7th Edition, 1993
Contributors:
B. Buchanan
S. Khresat
W. Lindemann
M. Pelletier-Hunyadi
P. Purves
P. Shelton
J. Vinson
B. Williams
T. Jones
B. McCaslin
TABLE OF CONTENTS
Chapter Page
1. Rocks and Minerals . . . . . . . . . . . . . . . . 2
2. Field Trip: Soil Formation . . . . . . . . . . . 7
3. Soil Sampling and Subsampling . . . . . . . . . . 12
4. Soil Texture . . . . . . . . . . . . . . . . . . 20
5. Soil Bulk Density and Particle Density . . . . . . 33
6. Field Trip: Soil Morphology . . . . . . . . . . . 40
7. Soil Colloids . . . . . . . . . . . . . . . . . . 48
8. Soil pH and Soluble Salts . . . . . . . . . . . . 57
9. Soil Water . . . . . . . . . . . . . . . . . . . 66
10. Water Movement in Soil . . . . . . . . . . . . . . 76
11. Soil Biology and Microbiology . . . . . . . . . . 82
12. Field Trip: Land use . . . . . . . . . . . . . . 87
13. Soil Fertility . . . . . . . . . . . . . . . . . 93
Chapter 1
ROCKS AND MINERALS
I. ROCKS
Rocks are aggregates of one or more minerals. There are three
classes of rocks based upon their formation mode. These are; Igneous,
Sedimentary, and Metamorphic.
IGNEOUS ROCKS: These rocks are formed from the
cooling and solidification of molten magma (volcanoes). They are
the most abundant rocks in the earth's crust. Igneous rocks are
classified on their chemical composition and mode of occurrence.
According to their chemical composition igneous rocks are
classified as follows. Acidic igneous rocks
contain more than 65 % silica and are usually light in color
(e.g. Granite). Basic igneous rocks contain less
than 50% silica and are usually dark colored (e.g. Basalt). Neutral
igneous rocks contain between 50 and 65% silica (e.g. Andesite).
According to their mode of occurrence (location of the rocks when
they were formed) igneous rocks are classified as follows.
Intrusive rocks have formed deep within the
earth's crust under a relatively slow cooling process and have
coarse textured grains (e.g. Granite, Gabbro). Extrusive
rocks have formed near the earth's surface under a relatively
rapid cooling process and have fine textured grains (e.g.
Rhyolite, Basalt).
SEDIMENTARY ROCKS. Sedimentary rocks are
classified as either clastics or precipitates.
Clastics are formed through physical means where
fragments or sediments of decaying igneous rocks are consolidated
into solid masses by pressure or cementing agents. The cementing
agents range from clay to calcium carbonate.(e.g. Limestone). The
precipitates are produced either by chemical or
biochemical precipitation of soluble ions from solution.
METAMORPHIC ROCKS. Metamorphic rocks are
classified on the basis of their structure and parent rock. Foliated
or banded metamorphic rocks have parallel layers of different
minerals. The color may be uniform or alternate between light and
dark colored layers (e.g. Slate). The non-foliated
or non-banded types have random patterns of minerals and colors
(e.g. Marble).
II. MINERALS
Minerals are naturally occurring inorganic substances which have
a certain chemical composition, distinctive physical properties,
and are classified according to these characteristics. Based upon
origin there are primary and secondary
minerals.
Primary minerals are formed at elevated temperatures from igneous and metamorphic rocks. They are present in the original rock form from which the soil was formed. (e.g. Feldspars).
Secondary minerals are formed in soil by decomposition of the primary minerals and their recomposition into new ones (e.g. Calcite).
Physical properties used in the identification of minerals are cleavage or fracture, color, streak, and hardness. Cleavage is the property of breaking along one or more smooth, parallel planes on the crystal axes of the mineral. Cleavage is described by the number of directions and the angle between cleavage surfaces. Some minerals break in directions other than along crystal axes forming regular patterns. This property is called fracture.
Streak is the color of the finely powdered mineral and is determined by rubbing the mineral on a piece of unglazed porcelain.
Hardness is the resistance that a mineral
offers to scratching or abrasion. Harder minerals weather more
slowly than softer minerals (see Moh's Scale of hardness of
Minerals).
Lab Exercise:
- Examine the samples of igneous rocks in the lab and determine
their properties--acidic or basic, extrusive or intrusive.
- Examine the samples of the sedimentary rocks and determine
their classification (clastics or precipitates).
- Examine the samples of the metamorphic rocks and determine
their structure.
- Examine the selected minerals in the lab. and determine their
physical properties, and chemical composition. (Use the
information in Table 1.1 to help you in studying the minerals).
MOH'S SCALE OF HARDNESS OF MINERALS
| No. | Mineral | Chemical Composition | Character |
| 1. | Talc | H2Mg3Si4O12 | Scratched by finger nail |
| 2. | Gypsum | CaSO4-2H2O | Thumbnail scratches |
| 3. | Calcite | CaCO3 | Penny scratches |
| 4. | Fluorite | CaF2 | Soft iron scratches |
| 5. | Apatite | Ca5(PO4) 3 (F, C1, OH) | Knife blade scratches |
| 6. | Orthoclase | KA1Si3O8 | Knife barely scratches |
| 7. | Quartz | SiO2 | Scratches glass, steel |
| 8. | Topaz | A12SiO-F2 | Scratches quartz |
| 9. | Corundum | Al2O3 | Scratches topaz |
| 10. | Diamond | C | Scratches corundum |
Study the selected minerals on the desks and determine their
physical properties, chemical composition, origin, and potential
supply of plant nutrient. Use the information in Table 1.1 your
text, and the mineralogy texts available in the laboratory to
assist in your study.
TABLE 1.1 CLASSIFICATION OF MINERALS
Chemical |
|
Fracture or |
Specific |
|
|
Name |
Compsition |
Hardness |
Cleavage |
Gravity |
Color |
| Feldspars | |||||
| 1. Orthoclase | KA1Si3O8 | 6.0-6.5 | C-2 at right | 2.56 | Flash Red |
| 2. Albite | NaAlSi3O8 | 6.0-6.5 | " " | 2.61 | White |
| 3. Anorthite | CaA12Si2O8 | 6.0-6.5 | " " | 2.75 | White |
| 4. Labradorite | (Ca, Na) A12Si2O8 | 6.0 | " " | 2.70 | Dark Gray |
| Amphiboles and Pyroxenes | |||||
| 1. Augite | (Ca, Mg, Fe) (Sio3)2 | 5.0-6.0 | C at 87o & 93o | 3.2-3.6 | Blackish Green |
| 2. Hornblende | (Ca, Mg, Fe) SiO3 | 5.0-6.0 | C at 55o & 125o | 2.9-3.4 | Black |
| Micas | |||||
| 1. Biotite | H2K(Mg, Fe)3(AlFe)SiO4)3 | 2.5-3.0 | C | 2.7-3.1 | Black |
| 2. Muscovite | H2KAl3(SiO4)3 | 2.0-2.25 | C | 2.76-3.00 | Colorless, Gray |
| Olivine | |||||
| 1. Olivine | (Mg, Fe)2SiO4 | 6.0-7.0 | F-** | 3.3-3.6 | Green |
| Hydrated Minerals | |||||
| 1. Talc | H2Mg3Si4O12 | 1.0-1.5 | C | 2.6-2.8 | White |
| 2. Kaolinite | H4Al2Si2O9 | 1.0-2.5 | F | 2.59 | White |
| 3. Chlorite | H8Mg5Al2Si3O18 | 1.0-2.5 | F | 2.6-3.0 | Green |
| 4. Bentonite | H6Al2Si4O14H2O | 1.5-2.5 | F | 2.3-2.7 | White-Gray |
| Carbonates | |||||
| 1. Calcite | CaCO3 | 3.0 | C-Perfect | 2.6-2.71 | Colorless |
| 2. Dolomite | CaMg(CO3)2 | 3.5-4.0 | C(poor) | 2.89-2.9 | White Gray |
| Oxides | |||||
| 1. Quartz | SiO2 | 7.0 | F | 2.65 | Colorless White |
| 2. Magnetite | Fe3O4 | 5.5-6.5 | F | 5.16-5.18 | Iron Black |
| 3. Hematite | Fe2O3 | 5.5-6.5 | F | 4.9-5.3 | Red to Black |
| 4. Limonite | 2Fe2O3 3H2O | 5.0-5.5 | F | 3.6-4.0 | Yellow |
| Sulphates | |||||
| 1. Satinspar | CaSO4 2H2O | 1.5-2.0 | C-Fibrous | 2.32 | White |
| 2. Selenite | CaSO4 2H2O | 1.5-2.0 | E-Fibrons | 2.32 | White |
| Sulfides | |||||
| 1. Pyrite | FeS2 | 6.0-6.5 | F | 4.95-5.10 | Yellow Brassy |
| 2. Galena | PbS | 2.5-2.7 | C-3 Cubical | 7.4-7.7 | Gray-Black |
| Chlorides | |||||
| 1. Halite | NaC1 | 2.5 | C-Cubic | 2.1-2.6 | Colorness White |
| Phosphates | |||||
| 1. Apatite | Ca5F(PO4)3 | 5.0 | C-(poor) | 3.17-3.23 | Green |